Tender For Gas Chromatography With Mass Spectrometry With Pyrolyzer And With Installation & Training

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Tender For Gas Chromatography With Mass Spectrometry With Pyrolyzer And With Installation & Training; Gas Chromatograph  The Gas Chromatograph that provides superior performance.  Capabilities for two inlets and three detectors can be installed including MS and operated simultaneously.  Easy access to Maintenance and Service modes system interface.  Retention time repeatability <0.008 %  Area repeatability <0.5 % RSD  Hands free leak check  System should have retention time locking capability/automatic adjustment of retention time/Retention time alignment.  The instrument must be supplied with any hydrocarbon if required for adjustment/alignment of retention time or retention time locking. Pressure/Flow control pneumatics  System must have EPC/AFC Control for all injectors & detectors.  Pressure setpoint and control precision to 0.001 psi  Pressure/flow ramps: Minimum three.  Pressure range 0-100psi or more. Browser interface  Touchscreen browser interface Auto Sampler Automated Liquid Sampler (ALS):  Two auto injectors with minimum 12 vials capacity each or better.  Must support 100μL syringes or more.  Should be quoted for 2μl vials. Multi-Shot Pyrolyzer A Multi-shot Pyrolyzer compatible with GCMS for Pyrolysis of various samples. The Pyrolyzer should be capable of doing Evolved Gas Analysis, Reactive Pyrolysis, Multistep Thermal Desorption and other advanced high temperature applications. Should meet below specifications:  The Pyrolyzer should have a small Vertical Furnace, with cylindrical ceramic heater.  Pyrolysis tube material should be Quartz.  Temperature range should be up to 1050ºC with 1C step and +- 0.1C stability.  Cooling of Furnace should be very fast- within 10 min for temperature to go down from 800ºC to 50ºC  Programing of Multi-step Pyrolysis should be possible.  Samples- solids, liquids and gases should be analyzed. Typically maximum capacity should be 50uL in sample cup.  Software to directly operate and control the Pyrolyser should be offered.  Below Standard set of accessories needs to be offered:  Quartz pyrolysis tube  2 Nos.  Ultra ALLOY capillary column  5% diphenyl 95% dimethylpolysiloxane, L=30 m (i.d.=0.25mm), df=0.25 μm–1 No.  Capillary tube for evolved gas analysis  (UADTM, deactivated tube, L=2.5 m, i.d.=0.15 mm) –1No  ITF needle N  2 Nos.(with one ITF union)  Eco cup  Eco cup (50 μL)- 20 Nos., Eco cup LF (80 μL)- 20 Nos.  Eco stick  Eco stick SF -10 Nos., Eco stick DF -10 Nos.  Liquid sampler -1 No., septum for liquid sampler 5 Nos.  Graphite Vespel ferrule  3 Nos. Oven  Column Oven can accommodate two columns with a temperature range from 5 °C to 400 °C.  Set point resolution of 0.1°C.  Must support minimum 15 ramps or more.  Maximum temperature ramp rate of 100 °C /min or better.  Cool down of Oven from 450 °C to 50 °C in 4 min or less. Inlets Split/Split less Injector (SSL Inlet) (2Qty):  One Split/Split less Injector (SSL) for split and split less.  Fully EPC controlled and pressure range up to 100 psi or more.  Maximum temperature should be 400 °C or more.  Split Ratio 9000:1 or more to avoid column overload.  Gas saver mode to reduce gas consumption without compromising performance. Detectors Flame Ionization Detector (FID):  Minimum detectable level (for dodacane/tridecane): <1.2 pg C/s or better  Minimum temperature should be 450 °C or more.  Linear dynamic range : 107 or better  Data rates up to 500 Hz or better.  Must have the Flameout detection and automatic reignition capability. Mass Spectrometry (MS)  Ionization modes: EI  No consumable ion source would be acceptable.  Mass range m/z: 1 to 1000 amu/u or more.  Ion source temperature: up to 300 °C or better.  Transfer line temperature: up to 350 °C or better.  EI-electron energy: 200 eV or better.  Emission current: up to 250µA  Quadrupole: heated/metallic quadrupole  Mass axis stability: ±0.1 amu/ u over 48 h or better.  Dynamic Range: 106 or better.  Mass resolution: Unit mass or better.  Scan rate: up to 15,000 u/sec or higher.  Dual EI filament for EI source.  Turbo molecular pumps, more than 250 L/sec or better.  EI scan for m/z 272 with 1µL of Octafluoronaphthalene (OFN) at 1pg/µL should be S/N 1500:1 or better.  EI Instrument Detection Limit (IDL): 10fg or better with 1µL of 100fg injection of OFN or better. Software  Original window-based software with license  MS Software for Acquisition, data handling (quantitative/qualitative) and reporting  Full scan and SIM scan. Automated SIM setup and synchronous SIM/scan operation.  Latest original licensed NIST library must be present. Computer  Windows: Windows 11 Professional, 64-bit  Processor: Intel core ultra 7, 5 GHz.  RAM: 16 GB, expandable DDR5 (5600 MHz)  Internal hard drive: 1 TB SSD  27-inch IPS monitor  In-built Wifi 6E/7 Printer  Branded colour All-in-one auto duplex with wifi. Consumables Liquid auto sampler Consumables:  Liquid auto sampler syringe 10µL- 12 Quantity  Liquid Vials with caps 2 ml- 5000 Quantity GC Consumables:  Inlet Septa- 400 Quantity  Liner O ring- 100 Quantity  Split Liners- 25 Quantity  Split less Liners- 25 Quantity  Glass wool- 10gm  Ferrules for 0.25 mm column ID- 100 Quantity  Ferrules for 0.32 mm column ID- 100 Quantity  Ferrules for 0.53 mm column ID- 100 Quantity  Column nut- 10 Quantity  Column cutter- 1 Quantity  Tubing cutter- 1 Quantity  FID Jet- 5 Quantity  GC installation kit- 1 Quantity  Inline helium trap filter- 1 Quantity  Split vent trap- 10 Quantity  Inlet seal- 10 Quantity MS Consumables:  EI Filament- 6 Quantity  EI tuning solution- 1 Quantity each  MS nut- 10 Quantity  MS cleaning tool kit- 1 Quantity  Vacuum pump oil- 5 L  MS Ferrules for 0.25 mm column ID- 100 Quantity  MS Ferrules for 0.32 mm column ID- 100 Quantity  MS Ferrules for 0.53 mm column ID- 100 Quantity  Oil mist filter- 2 Quantity Columns:  DB-5MS or equivalent capillary column 30m x 0.25mm x 0.25µm (1 Quantity)  DB-624 or equivalent capillary column 30m x 0.25mm x 0.25µm (1 Quantity)  DB-Wax or equivalent capillary column 30m x 0.25mm x 0.25µm (1 Quantity)  HP-88 or equivalent capillary column 100m x 0.25mm x 0.20µm (1 Quantity) Accessories Gas Cylinders:  Hydrogen gas cylinder with Gas Purification Panel and double stage regulator- 2 Quantity  Nitrogen gas cylinder with Gas Purification Panel and double stage regulator- 2 Quantity  Zero Air gas cylinder with Gas Purification Panel and double stage regulator- 2 Quantity  Helium gas cylinder with Gas Purification Panel and double stage regulator- 2 Quantity  Inclusive of fittings, tubings and installation-- 1 Quantity each UPS: 10kVA compatible online UPS with 60 minutes backup Warranty  Five years on instrument including PC, printer and UPS + CMC for 3 years. Assistance may be provided for shifting of equipment from one place to another within the BSIP premises. Warranty must be valid after shifting of equipment also. Tool Kit  One set of tool kit to be supplied along with equipment.