Gc-Ms Gc-Ms (Gas Chromatograph Coupled With High Performance Quadrupole Mass Spectrometer) , Gc-Ms (Gas Chromatograph- Mass Spectrometer) , Specifications: Advanced Gas Chromatograph Coupled With High Performance Quadrupole Mass Spectrometer With Automate, peechi-Kerala

Gc-Ms Gc-Ms (Gas Chromatograph Coupled With High Performance Quadrupole Mass Spectrometer) , Gc-Ms (Gas Chromatograph- Mass Spectrometer) , Specifications: Advanced Gas Chromatograph Coupled With High Performance Quadrupole Mass Spectrometer With Automated Liquid Injector & Headspace Sampler Requirement Specifications • General Features Of Gc • Peak Retention Time Repeatability: < 0.0008 Min. • Peak Area Repeatability: < 1% Rsd • Fully Automated With Gas Flow/Pressure Control Through Ppc/ Epc/Afc For Injector & Detector Gas. • System Should Have Capability To Install 3 Or More Independent Injection And Detector Ports. Column Oven • Operational Temperature Range: Ambient +2 To 450°C • Ramp Rate: Maximum 100°C/Min Or More • Cooling Rate: 450°C To 50°C Within 3.5 Min Or Better With Option Of User Specified Cooling Ramps • Built-In Oven Light That Facilitates Column Installation Should Be Available • Should Have Oven Power Safety. Split/Splitless Injector Port – 1 No • Split/Split Less Capillary Inlet • Maximum Temperature: 450 °C • Split Ratio: 9000:1 Or More • Pressure Setting Range 0– 150 Psi With Control Set Point Of 0.001Psi For Specified Pressure Range • Carrier Gas Flow Control Should Have Constant Flow, Constant Pressure Modes • Pressure/Flow Program Ramps: Minimum 5 Steps Flame Ionization Detector • Operating Temperature: 450?C • Minimum Detectable Level: < 1.2 C/S Or Better • Standard Pneumatic Control For Gas: Epc/Apc/Ppc Flow Control For H2 And Air And Controlled Through Software. • Linear Dynamic Range: > 107 • Flame Out Detection And Automatic Re-Ignition: Enable • Data Rate Set: Able To Set Data Rate Up To 500 Hz. Auto Injector • Inbuilt Autoinjector With Sample Vial Capacity Of 15 Or More • Area Reproducibility Better Than 0.5 % Rsd Using Multi-Component Standard • Syringe Up To 10 Ul As Standard Or Better • Sample Volume Injection Should Be In The Range Of 0.1 To 8.0 ?L Using 10Ul Syringe Headspace Sampler • Vial Tray:Must Have Minimum 80 Vials Capacity With Provision To Place 10 Ml, 20 Ml Vials. • Vial Incubator:Must Have 12 Vials Heated Independently In Overlapping Mode. • Oven Temp:Must Programmable Up To 340°C • Valve & Loop Temperature Must Have 280°C • Sample Line Temp: 218°C • Transfer Line: Must Have Less Than 40Cm And Coupling Connections Should Not Exposing To Atmospheric Conditions To Minimize Interference. • Carry Over < 0.15% • Loop: Stainless Steel Coated With Inert Material • Must Have Inert Sample Flow Line With 1Ml Sulfinet Sample Loop. • Leak Check: Must Have All Vial Automatic Check • Carrier Gas And Vial Pressurized Gas Control: Automated Flow/Pressure Controller. • Must Be A Single Software For Both Gc & Hs System. • Headspace & Auto Liquid Sampler Should Be Coupled To Gc System By Independent Channel To Reduce Cross-Contamination Gcms Instrument Should Built With Self-Diagnostic Features And Automated Tuning And Start-Up Tools For Better Productivity Single Quadruple Mass Spectrometer • Ionization Mode: Ei Ionization & System Should Have Dual Filament With Automatic Filament Switching. • Should Be Upgradeable To Ci Ionization. • Ion Source Temperature: Up To 350°C • Electron Energy Range Up To 200Ev Or Better • Electron Current Should Be 200Ua • Mass Range: 1.5 To 1000 Amu Or Better. • Mass Analyzer: Quadruple Should Be Made Up Of Solid Rugged Metal And Must Have The Pre-Filters Or Facility To Minimize The Influence Of Contamination. • Vacuum Pump: High Capacity Turbomolecular Pump 250 L/S And Above Capacity • Mass Axis Stability: ±0.1 Amu Over 48 Hours • Mass Resolution: Unit Mass • Detector: Sealed Long-Life Electron Multiplier Tube • Scan Rate: 20,000 Amu/S Or Better And Should Retain Sensitivity For All Available Scan Rates • Should Have Automatic Leak Check, Visualize Remaining Time For Stabilization Of Vacuum And Automatic Tuning Judgement Features. • Licensed Version Of Latest Wiley/Nist Mass Spectral Library Should Be Provided. • System Should Be Field Upgradeable To Direct Introduction Of Sample To Ms Ion Source System Bypassing Gc Without Removing Column In Gc Oven And Heat Able Up To 500?C At 5 Different Programming Speeds Ms Installation Checkout • Ei Scan Sensitivity: 2000:1 Or Higher For 1Pg Of Ofn At Nominal 272U Ion. • Instrument Detection Limit: Instrument Detection Limit On Ofn Should Be 10 Fg Or Better With The Injection Of 1 Ul Of 100 Fg/Ul Ofn Standard By Statistically Derived At 99 % Confidence Level From 8 Sequential Injection For M/Z 272 Using Standard Ms Column Supplied With Instrument. Software • Suitable Software For Data Acquisition, Qualitative & Quantitative Analysis Tools • Should Automatically Create Sim Ions From Acquired Scan Data And Optimizing Tool For Sim Group Creation With Dwell Time For Better Repeatability And Peak Profile. • Instrument Acquisition, Acquired Data Analysis And Reporting Should Have Been Built Based On The Compound Retention Indices Through Automated Features. Computer And Printer • Latest Configuration Branded Computer With Licensed Operating System Compatible With The Instrument Software For Smooth Operationsand Laser Printer (B/W, Double Side Printing) Gas Cylinders • One Each Cylinders (47 Lit) Filled Gas, Regulators, Gas Purification Panel, Tubing For Helium, Nitrogen, Hydrogen And Zero Air To Be Quoted Columns • Hp-5 Ms/ Db-5 Ms/ Rtx-5Sil Ms /Equivalent Type Capillary Column • Stable Wax Column Syringes • 2 Manual Syringes – 10 ?L Consumables • Ferrules, Septum’S, Glass Inserts, Ms Ion Source Filaments – 3 Nos Over 5 Years Duration. Warranty • Warranty For 5 Years Including Maintenance Kits

INR 9750 /-

INR 65000.0 /-

INR 65 Lakhs /-

Name of Work: Supply and Installation of GC-MS (Gas Chromatograph - Mass Spectrometer)

Sl. No.	Item Description
1	GC-MS (Gas Chromatograph- Mass Spectrometer)
2	Specifications: Advanced Gas Chromatograph coupled with high performance Quadrupole Mass Spectrometer with automated liquid injector & headspace sampler Requirement Specifications • General Features of GC • Peak retention time repeatability: < 0.0008 min. • Peak Area repeatability: < 1% RSD • Fully automated with gas flow/pressure control through PPC/ EPC/AFC for injector & Detector gas. • System should have capability to install 3 or more independent injection and detector ports. Column Oven • Operational Temperature Range: Ambient +2 to 450°C • Ramp rate: maximum 100°C/min or more • Cooling rate: 450°C to 50°C within 3.5 min or better with option of user specified cooling ramps • Built-in oven light that facilitates column installation should be available • Should have oven power safety. Split/Splitless injector port – 1 No • Split/split less capillary inlet • Maximum temperature: 450 °C • Split ratio: 9000:1 or more • Pressure setting range 0– 150 psi with control set point of 0.001psi for specified pressure range • Carrier gas Flow Control should have Constant flow, constant pressure modes • Pressure/Flow program ramps: minimum 5 steps Flame Ionization Detector • Operating temperature: 450?C • Minimum detectable level: < 1.2 C/s or better • Standard pneumatic control for gas: EPC/APC/PPC flow control for H2 and air and controlled through software. • Linear Dynamic Range: > 107 • Flame out detection and automatic re-ignition: Enable • Data rate Set: Able to set data rate up to 500 Hz. Auto Injector • Inbuilt autoinjector with sample vial capacity of 15 or more • Area reproducibility better than 0.5 % RSD using multi-component standard • Syringe up to 10 uL as standard or better • Sample volume injection should be in the range of 0.1 to 8.0 µl using 10uL syringe Headspace Sampler • Vial tray:must have minimum 80 Vials capacity with provision to place 10 ml, 20 ml vials. • Vial Incubator:must have 12 vials heated independently in overlapping mode. • Oven Temp:must programmable up to 340°C • Valve & loop temperature must have 280°C • Sample line Temp: 218°C • Transfer Line: must have less than 40cm and coupling connections should not exposing to atmospheric conditions to minimize interference. • Carry Over < 0.15% • Loop: Stainless steel coated with inert material • Must have inert sample flow line with 1mL sulfinet sample loop. • Leak Check: must have all vial automatic check • Carrier Gas and Vial pressurized gas Control: Automated Flow/pressure Controller. • Must be a single software for both GC & HS system. • Headspace & auto liquid sampler should be coupled to GC system by independent channel to reduce cross-contamination GCMS instrument should built with self-diagnostic features and automated tuning and start-up tools for better productivity Single Quadruple Mass Spectrometer • Ionization mode: EI ionization & System should have dual filament with automatic filament switching. • Should be upgradeable to CI ionization. • Ion Source temperature: up to 350°C • Electron energy range up to 200eV or better • Electron current should be 200uA • Mass Range: 1.5 to 1000 amu or better. • Mass analyzer: Quadruple should be made up of solid rugged metal and must have the pre-filters or facility to minimize the influence of contamination. • Vacuum pump: High capacity turbomolecular pump 250 L/s and above capacity • Mass axis stability: ±0.1 amu over 48 hours • Mass resolution: Unit mass • Detector: Sealed long-life electron multiplier tube • Scan rate: 20,000 amu/s or better and should retain sensitivity for all available scan rates • Should have Automatic leak check, Visualize remaining time for stabilization of vacuum and Automatic tuning judgement features. • Licensed version of latest Wiley/NIST Mass Spectral Library should be provided. • System should be field upgradeable to direct introduction of sample to MS ion source system bypassing GC without removing column in GC oven and heat able up to 500?C at 5 different programming speeds MS installation checkout • EI Scan Sensitivity: 2000:1 or higher for 1pg of OFN at nominal 272u ion. • Instrument detection limit: Instrument detection limit on OFN should be 10 fg or better with the injection of 1 ul of 100 fg/ul OFN standard by statistically derived at 99 % confidence level from 8 sequential injection for m/z 272 using standard MS column supplied with instrument. Software • Suitable software for data acquisition, qualitative & quantitative analysis tools • Should automatically create SIM ions from acquired Scan data and optimizing tool for SIM group creation with dwell time for better repeatability and peak profile. • Instrument acquisition, acquired data analysis and reporting should have been built based on the compound retention indices through automated features. Computer and printer • Latest configuration branded computer with licensed operating system compatible with the instrument software for smooth operationsand Laser printer (B/W, double side printing) Gas Cylinders • One each cylinders (47 Lit) filled gas, regulators, gas purification panel, tubing for Helium, Nitrogen, Hydrogen and zero air to be quoted Columns • HP-5 MS/ DB-5 MS/ Rtx-5Sil MS /equivalent type capillary column • Stable Wax column Syringes • 2 Manual syringes – 10 µl Consumables • Ferrules, septum’s, glass inserts, MS ion source filaments – 3 Nos over 5 years duration. Warranty • Warranty for 5 years including maintenance kits